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imidazole

5-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]pentyl methanesulfonate

→

4-[4-[5-(1-imidazolyl)pentyl]phenoxymethyl]-2-[(E)-2-phenylethenyl]oxazole

수율 66.0%

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실험 절차

In substantially the same manner as in Working Example 8, imidazole was allowed to react with 5-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]pentyl methanesulfonate to give 4-[4-[5-(1-imidazolyl)pentyl]phenoxymethyl]-2-[(E)-2-phenylethenyl]oxazole. The yield was 66%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 101-102° C.

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