반응 #40832

반응 방정식

triethylaluminum

ethyl 5,6-diphenylpyridine-2-carboxylate

Compound 21

ethyl 5,6-diphenylpyridine-2-carboxylate

N,N′-dimethylethylenediamine

→

title compound

1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one

용매

toluene

반응 조건

후처리

1. 1
   기타were reacted

실험 절차

Following General Procedure O, ethyl 5,6-diphenylpyridine-2-carboxylate (Compound 21, 267 mg, 0.81 mmol) in toluene (5 ml), N,N′-dimethylethylenediamine (DMEDA, 85 mg, 0.97 mmol) and triethylaluminum (2.6 ml, 2.64 mmol, 1 M in hexane) were reacted to give the title compound as a yellow solid.

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