반응 #40301

반응 방정식

4,4-dimethyl-cyclohex-2-enone

hydrogen

→

4,4-dimethyl-cyclohexanone

수율 94.0%

용매

ethyl acetate

반응 조건

후처리

1. 1
   여과Filtration over celite
2. 2
   농축concentration
3. 3
   기타by evaporation

실험 절차

A solution of 4,4-dimethyl-cyclohex-2-enone (3 mmol) in ethyl acetate is hydrogenated overnight at room temperature using Pd/C (0.05 mmol) with hydrogen under normal pressure. Filtration over celite and then concentration by evaporation produces 4,4-dimethyl-cyclohexanone (355 mg) in a yield of 94% (J. Org. Chem. 2001, 66 (3), 733-738).

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