반응 #40284

반응 방정식

N-Boc-β-alanine

propargyl alcohol

Dicyclohexyl-carbodiimide

→

N-Boc-β-alanine Propargyl Ester

용매

EtOAc

반응 조건

후처리

1. 1
   여과the reaction mixture was filtered
2. 2
   기타evaporated to dryness under vacuum
3. 3
   기타Crude product yield

실험 절차

N-Boc-β-alanine (1.91 g, 10.1 mmol) and propargyl alcohol (0.675 g, 12 mmol) were dissolved in EtOAc (25 mL). Dicyclohexyl-carbodiimide (DCC, 2.06 g, 10 mmol) was added to the solution and after 16 h of stirring at room temperature, the reaction mixture was filtered and evaporated to dryness under vacuum. Crude product yield

출처