반응 #3837

반응 방정식

4-(3-oxo-3H-benzo[d]isothiazol-2-yl)benzenesulfonamide

2-mercapto-propionylglycine

→

title compound

수율 92.3%

{2-[2-(4-Sulfamoylphenylcarbamoyl)phenyldisulfanyl]propionylamino}-acetic acid

수율 92.3%

반응 조건

후처리

1. 1
   기타This compound was prepared
2. 2
   세척The product was washed with ether
3. 3
   기타dried in vacuo

실험 절차

This compound was prepared according to the method of Example 132 using 0.46 g (1.5 mmol) of 4-(3-oxo-3H-benzo[d]isothiazol-2-yl)benzenesulfonamide and 0.25 g (1.5 mmol) of 2-mercapto-propionylglycine. The product was washed with ether and dried in vacuo to give 0.65 g of the title compound, mp 254°-256° C.

출처