반응 #3832
ord-3891158d65564d66834bcdc1c2f37155
반응 방정식
2,2'-dithiobisbenzoyl chloride
cyclopropylamine
triethylamine
dichloromethane
dichloromethane
→
title compound
2,2'-Dithiobis(N-cyclopropylbenzamide)
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타A solid formed immediately
- 2여과filtered
- 3기타The solid was dried
실험 절차
A solution of 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 20 mL of dichloromethane was added dropwise to a solution of cyclopropylamine (0.52 mL, 7.5 mmol) and triethylamine (1.2 mL, 9.0 mmol) in 20 mL of dichloromethane. A solid formed immediately, the mixture was stirred for 3 hours and then filtered. The solid was dried to yield 0.65 g of the title compound, mp 257°-259° C.;