반응 #3808

반응 방정식

2,2'-dithiobisbenzoyl chloride

4-nitro-3-(trifluoromethyl)aniline

→

title compound

수율 6.3%

2,2'-Dithiobis[N-[4-nitro-3-(trifluoromethyl)phenyl]benzamide]

수율 6.3%

용매

pyridine

dichloromethane

반응 조건

후처리

1. 1
   기타This compound was prepared
2. 2
   기타The crude product was recrystallized from ethyl ether

실험 절차

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 4-nitro-3-(trifluoromethyl)aniline (2.39 g, 11.6 mmol) in 19 mL of pyridine. The crude product was recrystallized from ethyl ether to yield 0.25 g of the title compound, mp 167°-169° C.

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