반응 #3792

반응 방정식

2,2'-dithiobisbenzoyl chloride

4-amino-N-(2-pyrimidinyl) benzenesulfonamide

→

title compound

수율 58.2%

2,2'-Dithiobis[N-[4-[(2-pyrimidinylamino)sulfonyl]phenyl]-benzamide]

수율 58.2%

용매

pyridine

dichloromethane

반응 조건

후처리

1. 1
   기타This compound was prepared
2. 2
   기타The crude product was recrystallized from a mixture of dimethylformamide, ethanol, and water

실험 절차

This compound was prepared according to the general methods described in Example 1 using 2,2'-dithiobisbenzoyl chloride (3.0 g, 8.7 mmol) in 30 mL dichloromethane and 4-amino-N-(2-pyrimidinyl) benzenesulfonamide (5.3 g, 21.7 mmol) in 100 mL pyridine. The crude product was recrystallized from a mixture of dimethylformamide, ethanol, and water to yield 3.9 g of the title compound, mp 280° C.

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