반응 #3742

반응 방정식

2, 3-dicyano-pyrazine

isobutylene

sulfuric acid

→

N-tert-butyl-2-pyrazinecarboxamide

3-cyano-N-tert-butyl-2-pyrazinecarboxamide

용매

tert-butyl alcohol

반응 조건

후처리

1. 1
   기타can be obtained

실험 절차

A compound having the formula (4) can be obtained as follows. The corresponding 2, 3-dicyano-pyrazine is reacted with tert-butyl alcohol or isobutylene in the presence of sulfuric acid to obtain the corresponding N-tert-butyl-2-pyrazinecarboxamide and/or 3-cyano-N-tert-butyl-2-pyrazinecarboxamide. Then, thus obtained corresponding N-tert-butyl-2-pyrazinecarboxamide and/or 3-cyano-N-tert-butyl-2-pyrazinecarboxamide are hydrolyzed under an alkaline condition.

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