반응 #367690
ord-bc6187862d6e41b7a7c4d2fedb6c0ebe
반응 방정식
glutamine
(S)-glutamine
methanol
water
acetonitrile
→
(R)-glutamine
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Example 1 was repeated with the difference that the sample to be tested was a glutamine of unknown enantiomer composition, the comparison samples were (RS)-, (R)-, and (S)-glutamine, and the mobile phase was a mixture of methanol, water, acetonitrile, and tetrahydrofuran in a 1:1:2:2 ratio by volume. In this case, the (R)-glutamine gave a spot with an Rf -value of 0.70 and the (S)-glutamine gave a spot with an Rf -value of 0.62.