반응 #367497

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phenylglyoxal

2-(4-methylphenyl)-1,1-dimethylethanamine

→

title compound

N-(2-(4-Methylphenyl)-1,1-dimethylethyl)-2-hydroxy-2-phenyl ethanamine

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후처리

1. 1
   기타The title compound was prepared in the manner
2. 2
   기타The chromatographed material was recrystallized from cyclohexane

실험 절차

The title compound was prepared in the manner described in Example 9 using phenylglyoxal and 2-(4-methylphenyl)-1,1-dimethylethanamine. The chromatographed material was recrystallized from cyclohexane to give the title compound m.p. 137. τ(CDCl3 +d6DMSO) 8.95 (6H, s), 7.7 (3H, s), 7.35 (2H, s), 7.0-7.3 (2H, dd), 5.3 (1H, dd), 2.9 (4H, s), 2.5-2.7 (5H, m).

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