반응 #366620
ord-550de413773c49dd9b5b621e9b040826
반응 방정식
15-crown-5
phenylchloroformate
sodium fluoride
→
Phenylfluoroformate
반응 조건
온도
40°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타Reaction completion
실험 절차
To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).