반응 #3564

반응 방정식

2,4,6-trimethyl-benzyl cyanide

2,4-diamino-5-pyrimidine-carboxaldehyde

ammonia

→

title compound

6-(2,4,6-Trimethyl-phenyl)-pyrido[2,3-d]pyrimidine-2,7-diamine

용매

methane

반응 조건

실험 절차

The title compound was prepared according to Example 1, starting from 0.915 g of 2,4,6-trimethyl-benzyl cyanide and 0.76 g of 2,4-diamino-5-pyrimidine-carboxaldehyde; mp 276°-282° C.; CIMS (1% ammonia in methane): m/z (relative intensity) 279 (MH+, 54), 280 (MH+ +1, 100).

출처