반응 #353232

ord-d3e7d920830c495f938c2d13386767bf

반응 방정식

O=C(Cl)c1ccc(Br)cc1
parabromobenzoyl chloride
C#CCCCC
1-hexyne
CCCCC#CC(=O)c1ccc(Br)cc1
1-(4-bromophenyl) 2-heptyn-1-one

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The following were stirred at ambient temperature for about 2 hours 30 minutes, 49 ml of 1-hexyne, 75 ml of triethylamine, 40 mg of cuprous iodide, 40 mg of bis triphenylphosphine palladium dichloride and 9 g of parabromobenzoyl chloride.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05650414uspto-grants-1997_07