반응 #350556

반응 방정식

phthalonitrile

gallium trimethoxide

→

gallium phthalocyanine

용매

ethylene glycol

반응 조건

후처리

1. 1
   여과The resulting product was then filtered
2. 2
   세척The product was washed with N,N-dimethylformamide
3. 3
   건조with methanol, and then dried

실험 절차

31.8 parts of phthalonitrile, 10.1 parts of gallium trimethoxide, and 150 ml of ethylene glycol were stirred at a temperature of 200° C. in an atmosphere of nitrogen for 24 hours. The resulting product was then filtered. The product was washed with N,N-dimethylformamide and then with methanol, and then dried to obtain 25.1 parts of gallium phthalocyanine.

출처