반응 #350550

반응 방정식

quinoline

toluene

→

Naphthalene

반응 조건

후처리

1. 1
   기타After the reaction
2. 2
   기타the catalyst was recovered in a gas state
3. 3
   기타a low boiling point component was removed
4. 4
   기타to obtain a pitch
5. 5
   기타was 176° C.

실험 절차

Naphthalene was polymerized at a temperature of from 200° to 300° C. in the presence of a HF·BF3 catalyst. After the reaction, the catalyst was recovered in a gas state, and a low boiling point component was removed to obtain a pitch. The optically anisotropic phase was 2 volume % as observed under a polarization microscope, the softening point was 176° C., the quinoline-insoluble content was 1.6% by weight, and the toluene-insoluble content was 34% by weight.

출처