반응 #347219

반응 방정식

1,3-dipropyl-5,6-diaminouracil

1-adamantaneacetic acid

1-ethyl-3-(3-dimethylaminopropyl)carbodiimide

→

6-amino-5-(adamantan-1-yl)acetylamino-1,3-dipropyluracil

수율 112.8%

반응 조건

후처리

1. 1
   기타condensed

실험 절차

At first 2.00 g (8.85 mmol) of 1,3-dipropyl-5,6-diaminouracil and 2.06 g (10.6 mmol) of 1-adamantaneacetic acid were condensed according to the procedure of Example 1 using 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide to afford 4.02 g (yield: 100%) of amorphous 6-amino-5-(adamantan-1-yl)acetylamino-1,3-dipropyluracil as a crude product.

출처