반응 #346374

반응 방정식

cresol

NaOH

2-ethyl-1-hexanol

→

Sodium Cresolate

용매

xylene

반응 조건

후처리

1. 1
   기타A five liter flask was equipped with a stirrer
2. 2
   온도heating mantle, Dean-Stark trap and a reflux condenser
3. 3
   온도The batch was heated
4. 4
   온도to reflux
5. 5
   기타to collect the water

실험 절차

A five liter flask was equipped with a stirrer, thermometer dropping funnel, heating mantle, Dean-Stark trap and a reflux condenser. 329 grams of a 48.6% aqueous solution of NaOH was added to the flask along with 2000 ml of a 4:1 mixture of xylene and 2-ethyl-1-hexanol. 433 grams of commercial cresol (99.4% pure) was slowly added. The batch was heated to reflux to collect the water. The product was a solution of sodium cresolate:xylene-2-ethyl-1-hexanol mixture.

출처