반응 #344628

ord-685d9e8a1acb4944b57536da41f08daa

반응 방정식

ClC1=C(c2ccon2)CNCC1.O=C(O)C(=O)O
4-Chloro-3-(3-isoxazolyl)-1,2,5,6-tetrahydropyridine oxalate
CCOC1CC(C2=C(Cl)CCN(C(=O)c3ccccc3)C2)=NO1
1-benzoyl-4-chloro-3-(5-ethoxy-4,5-dihydro-3-isoxazolyl)-1,2,5,6-tetrahydropyridine
→
COCc1cc(C2=C(Cl)CCNC2)no1.O=C(O)C(=O)O
4-Chloro-3-(5-methoxymethyl-3-isoxazolyl)-1,2,5,6-tetrahydropyridine oxalate

반응물

ClC1=C(c2ccon2)CNCC1.O=C(O)C(=O)O
4-Chloro-3-(3-isoxazolyl)-1,2,5,6-tetrahydropyridine oxalate
CCOC1CC(C2=C(Cl)CCN(C(=O)c3ccccc3)C2)=NO1
1-benzoyl-4-chloro-3-(5-ethoxy-4,5-dihydro-3-isoxazolyl)-1,2,5,6-tetrahydropyridine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

4-Chloro-3-(3-isoxazolyl)-1,2,5,6-tetrahydropyridine oxalate starting from 1-benzoyl-4-chloro-3-(5-ethoxy-4,5-dihydro-3-isoxazolyl)-1,2,5,6-tetrahydropyridine. M.p. 195°-196° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05262427uspto-grants-1993_11