반응 #343051

ord-5725cf4fdc4c41cf9e1bff8f0e584847

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In the first process step, glucose (a) is reacted with octadecylamine (b) to give N-octadecyl-β-D-glucopyranosylamine (c) which is acylated in the second process step with oleoyl chloride to give N-octadecyl-N-oleoyl β-D-glycopyranosylamine (d). In the third process step, O-sulphonylation is then carried out in position 6 with methanesulphonyl chloride and N-octadecyl-N-oleoyl-(6-O-methylsulphonyl-β-D-glycopyranosyl)-amine (I) is obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04699899uspto-grants-1987_10