반응 #339549

반응 방정식

acetic acid 4-(4-methoxy-butyl)-pyridin-3-yl ester

diethyl ether pentane

→

title compound

4-(4-Methoxy-butyl)-pyridin-3-ol

용매

acetic acid

반응 조건

후처리

1. 1
   온도After cooling
2. 2
   여과the precipitate is collected by filtration

실험 절차

A mixture of 39 mmol acetic acid 4-(4-methoxy-butyl)-pyridin-3-yl ester in 20 ml acetic acid is heated to 70° C. for 30 minutes. After cooling, 75 ml of diethyl ether/pentane (1:5) is added and the precipitate is collected by filtration. The title compound is obtained from the solid by re-crystallization from toluene and identified based on its Rf value.

출처