반응 #335765
ord-929d79cd629e4e0098ad4a0e47eae538
반응 방정식
monochloroacetic acid
1,4-dichlorobenzene
chlorosulfonic acid
2,5-dichlorothiophenol
→
2,5-dichlorophenylthioglycolic acid
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
the method in which 1,4-dichlorobenzene is sulfochlorinated with chlorosulfonic acid and then reduced to 2,5-dichlorothiophenol with zinc powder under acidic conditions, followed by reaction with monochloroacetic acid to yield 2,5-dichlorophenylthioglycolic acid (U.S. Pat. No. 3,440,288),