반응 #335347

반응 방정식

hexadecanol

dimethylaminopyridine

ethyl 2-bromomethyl-2-propenoate

→

desired product

Ethyl 2-[(hexadecyloxy]methyl]-2-propenoate

용매

methylene chloride

반응 조건

후처리

1. 1
   기타The solvent is evaporated

실험 절차

To a stirred solution of 1.9 g of hexadecanol in 40 ml of methylene chloride containing 700 mg of dimethylaminopyridine is added 500 mg of ethyl 2-bromomethyl-2-propenoate followed by continued stirring for 18 hours. The solvent is evaporated to give 2.4 g of the desired product.

출처