반응 #335342
ord-1b159444d1244d48bc290c258391c5e9
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the solvent is removed
- 2기타the residue evaporated with toluene several times
실험 절차
To a moisture protected solution of 28.4 ml of phosphorous oxychloride in 200 ml of carbon tetrachloride is added dropwise with stirring a solution of 50 g of 1-hexadecanol in 125 ml of carbon tetrachloride. After stirring at ambient temperature for 18 hours, the solvent is removed and the residue evaporated with toluene several times to give 71 g of the desired product as a vacuum dried water white oil.