반응 #335320

반응 방정식

1-hexadecanol

2-[(acetyloxy)methyl]-2-propenoic acid, ethyl ester

dimethylaminopyridine

→

desired compound

수율 39.3%

(Hexadecyloxylmethyl]-2-propenoic acid, ethyl ester

수율 39.3%

용매

dichloromethane

반응 조건

후처리

1. 1
   기타the solvent is evaporated

실험 절차

To a mixture of 1.1 g of 1-hexadecanol and 400 mg of 2-[(acetyloxy)methyl]-2-propenoic acid, ethyl ester in 15 ml of dichloromethane is added 550 mg of dimethylaminopyridine. This mixture is stirred overnight, then the solvent is evaporated and the residue subjected to preparative tlc (25% ethyl acetate/petroleum ether), to give 324 mg of the desired compound.

출처