반응 #335006

ord-582a8a39dcd348d195f6f383bef92f05

반응 방정식

CC(C)c1cccc(C(C)C)c1NC(=O)CP(=O)(O)c1ccccc1
(±)-[2-[[2,6-bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phenyl phosphinic acid
CCCCCCCCCCCCO
1-dodecanol
CCCCCCCCCCCCOP(=O)(CC(=O)Nc1c(C(C)C)cccc1C(C)C)c1ccccc1
title compound
CCCCCCCCCCCCOP(=O)(CC(=O)Nc1c(C(C)C)cccc1C(C)C)c1ccccc1
(±)-[2-[[2,6-Bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phenylphosphinic Acid, Dodecyl Ester

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In a process analogous to Example 7, using (±)-[2-[[2,6-bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phenyl phosphinic acid in place of (±)-[2-[[2,6-bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phosphonic acid, ethyl ester and 1-dodecanol in place of 1-nonanol, the title compound is obtained as a sticky white solid; mp 66°-68° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05208224uspto-grants-1993_05