반응 #334978

반응 방정식

n-decyl alcohol

naphthalene-2,6-dicarboxylic acid dichloride

triethylamine

dimethylaminopyridine

→

titled compound

수율 56.3%

2-n-decyloxycarbonylnaphthalene-6-carboxylic acid chloride

수율 56.3%

용매

methylene chloride

반응 조건

후처리

1. 1
   workup.DISTILLATIONthe solution was distilled
2. 2
   기타to remove the solvent

실험 절차

After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.

출처