반응 #334893
ord-c5ec0c86aed749d4b5901138bf25d1f3
반응 방정식
ethylene carbonate
→
ethylene carbonate
수율 98.0%
carbon dioxide
수율 10.8%
반응 조건
온도
175°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도is heated
실험 절차
A 10:1 mole ratio of ethylene carbonate to polyglycol P-425 is heated with stirring under a nitrogen atmosphere for 6 hours at 175° C. using 0.5 percent sodium stannate trihydrate as catalyst to give 98 percent ethylene carbonate conversion to a poly(alkylene carbonate) polyol with 10.8 percent carbon dioxide. The catalyst is removed as in Example 1.