반응 #334888

ord-8a7eca64f5a648ddb4117baf4d3ae293

반응 방정식

O=C1OCCO1
ethylene carbonate
O=C1OCCO1
ethylene carbonate
수율 95.7%
O=C=O
carbon dioxide
수율 21.8%

반응 조건

온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

A 15:1 mole ratio of ethylene carbonate:diethylene glycol is heated with stirring under a nitrogen atmosphere for 8 hours at 150° C. using 1.0 percent Na2SnO3.3H2O as catalyst to give 95.7 percent ethylene carbonate conversion to a poly(alkylene carbonate) polyol with 21.8 percent carbon dioxide.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04709069uspto-grants-1987_11