반응 #334230
ord-a6a24a38902a493384f6355e7d0a9614
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.WAITare run in25 minutes
실험 절차
Into a solution under reflux of 50 g (0.424 mole) of 3,5 dimethylpiperidine at 96% in 60 ml benzene are run in25 minutes 22 g (0.212 mole) of 4-chlorobutyronitrile and the reflux is continued for 2h.