반응 #334230

ord-a6a24a38902a493384f6355e7d0a9614

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.WAITare run in25 minutes

실험 절차

Into a solution under reflux of 50 g (0.424 mole) of 3,5 dimethylpiperidine at 96% in 60 ml benzene are run in25 minutes 22 g (0.212 mole) of 4-chlorobutyronitrile and the reflux is continued for 2h.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04705795uspto-grants-1987_11