반응 #327979

반응 방정식

Ethynyltributylstannane

benzyl azide

→

title compound

1-benzyl-4-(tributylstannyl)-1H-1,2,3-triazole

반응 조건

후처리

1. 1
   기타purified by silica gel chromatography
2. 2
   세척eluting with 1:4 ethyl acetate

실험 절차

Ethynyltributylstannane (1 mL, 3.4 mmol) and benzyl azide (0.65 mL, 5.2 mmol) were heated to 130° C. for 24 hours. The mixture was adsorbed onto silica gel, and purified by silica gel chromatography eluting with 1:4 ethyl acetate:hexanes to afford the title compound.

출처