반응 #327943

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Phenylethynyltri-n-butyltin

benzyl azide

→

title compound

1-Benzyl-5-phenyl-4-(tributylstannyl)-1H-1,2,3-triazole

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후처리

1. 1
   기타The mixture was purified by silica gel chromatography
2. 2
   세척eluting with a gradient of 5-40% ethyl acetate in hexanes

실험 절차

Phenylethynyltri-n-butyltin (8.25 g, 21.1 mmol) and benzyl azide (2.3 mL, 18.4 mmol) were combined and heated to 150° C. overnight. The mixture was purified by silica gel chromatography eluting with a gradient of 5-40% ethyl acetate in hexanes to afford the title compound. MS (ESI+) m/z 526.3 (M+H)+.

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