반응 #3279

ord-3649f27493174d968301ce7cf9e817e4

반응 방정식

CSc1ncc2cc(-c3c(Cl)cccc3Cl)c(=O)n(C)c2n1
6-(2,6-dichlorophenyl)-8-methyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one
CSc1ncc2cc(-c3c(Cl)cccc3Cl)c(=O)n(C)c2n1
6-(2,6-Dichlorophenyl)-8-methyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one
CNC
dimethylamine
CN(C)c1ncc2cc(-c3c(Cl)cccc3Cl)c(=O)n(C)c2n1
6-(2,6-Dichlorophenyl)-2-dimethylamino-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-one

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound was prepared by a procedure similar to

실험 절차

This compound was prepared by a procedure similar to that described in Example 40 starting with 6-(2,6-dichlorophenyl)-8-methyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one of Example 37 and dimethylamine gas; mp 256°-258° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05733914uspto-grants-1998_03