반응 #323095
ord-9c8142fe5b77408a95c394638adc8152
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타(3 hours)
- 2기타the resulting precipitate is recrystallised from ethanol
실험 절차
80.8 parts of isatoic anhydride are introduced into 125 parts of dimethylacetamide, and a solution of 134.7 parts of stearylamine in 50 parts of dimethylformamide is added dropwise. When the evolution of CO2 has ended (3 hours) the resulting clear solution is stirred into 2 liters of H2O and the resulting precipitate is recrystallised from ethanol, using active charcoal. Anthranilic acid stearylamide of melting point 89°-90° C. is obtained.