반응 #322797

ord-eaffe5b65b4549bc95a3972b3bc260a7

반응 방정식

Cl.NNC(N)=O
hydrochloric acid semicarbazide
CC(=O)C(=O)O
pyruvic acid
CC(=NNC(N)=O)C(=O)O
2-carbamoylhydrazonopropionic acid

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Precipitated crystals
  2. 2
    여과were filtered out
  3. 3
    세척washed
  4. 4
    기타dried

실험 절차

22.3 g of hydrochloric acid semicarbazide was dissolved in 100 ml of water, and 13.9 ml of pyruvic acid was added to the solution while stirring. Precipitated crystals were filtered out, washed, and dried to obtain 21 g of 2-carbamoylhydrazonopropionic acid having a melting point of 201° C. (decomposed).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04640892uspto-grants-1987_02