반응 #320993

ord-02d78a39b61044aab1ed8219bd2e5b62

반응 방정식

NS(=O)(=O)c1ccc2c(c1)CCCC2
5,6,7,8-tetrahydro-2-naphthalenesulfonamide
O=C=Nc1ccc(Cl)cc1
4-chlorophenylisocyanate
→
O=C(Nc1ccc(Cl)cc1)NS(=O)(=O)c1ccc2c(c1)CCCC2
title compound
수율 56.0%
O=C(Nc1ccc(Cl)cc1)NS(=O)(=O)c1ccc2c(c1)CCCC2
N-([(4-chlorophenyl)amino]carbonyl)-5,6,7,8-tetrahydro-2-naphthalene sulfonamide
수율 56.0%

반응물

NS(=O)(=O)c1ccc2c(c1)CCCC2
5,6,7,8-tetrahydro-2-naphthalenesulfonamide
O=C=Nc1ccc(Cl)cc1
4-chlorophenylisocyanate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound was prepared by the method of Example 1 in 56% yield from 5,6,7,8-tetrahydro-2-naphthalenesulfonamide and 4-chlorophenylisocyanate, m.p. 163°-165° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05594028uspto-grants-1997_01