반응 #319836

반응 방정식

6-methyl-2,3,4,5-tetrafluorobenzoic acid

chloride

→

6-methyl-2,3,4,5-tetrafluorobenzoyl chloride

반응 조건

후처리

1. 1
   온도the mixture is refluxed for 1 hour
2. 2
   농축After concentrating

실험 절차

To 6-methyl-2,3,4,5-tetrafluorobenzoic acid (5.60 g) is added thiony chloride (9.8 ml) and the mixture is refluxed for 1 hour. After concentrating, 6-methyl-2,3,4,5-tetrafluorobenzoyl chloride (5.20 g) is obtained as a colorless oil, b.p. 82° C./23 mmHg.

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