반응 #316621
ord-d5049d1cc90a43e491ff842861e10a18
반응 방정식
용매
반응 조건
온도
75°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1추출Extraction and chromatography
실험 절차
A mixture of diethyl 5-iodo-2-furanphosphonate (1 mmol), 4-fluorophenylboronic acid (2 mmol), diisopropylethylamine (DIEA) (4 mmol) and bis(acetonitrile)dichloropalladium(II) (0.05 mmol) in 6 mL DMF was heated at 75° C. for 16 h. Extraction and chromatography provided diethyl 5-(4-fluorophenyl)-2-furanphosphonate as an oil.