반응 #316491

반응 방정식

phosgene

tetradecyl alcohol

→

product

수율 98.7%

Tetradecyl Chloroformate

수율 98.7%

용매

toluene

반응 조건

후처리

1. 1
   workup.WAITthe reaction mixture was left
2. 2
   기타After solvent evaporation
3. 3
   기타evaporated to dryness (several times)

실험 절차

29 ml of a 20% toluene solution of phosgene (55.98 mmoles) was added to tetradecyl alcohol (4 g, 18.66 mmoles) and the reaction mixture was left to stand for 20 hours under stirring at room temperature. After solvent evaporation, the residue was taken up with hexane and evaporated to dryness (several times) to give 5.1 g product as colourless liquid.

출처