반응 #312586
ord-ea8c19d0e5e54c419d16d402346fc712
반응 방정식
thioanisole
dimethyl sulfate
water
→
dimethylphenylsulfonium sulfate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타separated into two layers
실험 절차
6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium sulfate.