반응 #312258

ord-30945ee08e18440b9cf5a2a3418fa7aa

반응 방정식

CCCCCC(=O)Cl
hexanoyl chloride
C#C
acetylene
[Al+3].[Cl-].[Cl-].[Cl-]
aluminum chloride
CCCCCC(=O)C=CCl
1-chloro-1-octen-3-one
수율 94.0%

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound is prepared

실험 절차

This compound is prepared according to the procedure of Price and Pappalardo [C. C. Price and J. A. Pappalardo, Org. Syn, 32, 27 (1952)] from hexanoyl chloride, acetylene, and aluminum chloride in 94% yield, bp 51°-52° C. (0.1 mm); λ max 1680, 1595, 941 cm-1.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04235797uspto-grants-1980_11