반응 #312216
ord-0e0c9f328fc14207a0f5b0bbce5340c2
용매
반응 조건
온도
50°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타titer 53° C.
- 2workup.WAITfollowed by 60 minutes of agitation at 70° C
- 3여과The hollow formed granulate is filtered
- 4기타dried
실험 절차
100 of myristic acid which has been granulated from an aqueous emulsion as described in Example 1 (AN 246, titer 53° C. particle size 0.2-0.3 mm.) and 60.2 g strontium hydroxide octahydrate (97% active) are suspended in one liter of water at 50° C. temperature and stirred for 30 minutes at 50° C. followed by 60 minutes of agitation at 70° C. The hollow formed granulate is filtered and dried. The content of free fatty acid amounts to 1.7%.