반응 #312216

ord-0e0c9f328fc14207a0f5b0bbce5340c2

용매

반응 조건

온도
50°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타titer 53° C.
  2. 2
    workup.WAITfollowed by 60 minutes of agitation at 70° C
  3. 3
    여과The hollow formed granulate is filtered
  4. 4
    기타dried

실험 절차

100 of myristic acid which has been granulated from an aqueous emulsion as described in Example 1 (AN 246, titer 53° C. particle size 0.2-0.3 mm.) and 60.2 g strontium hydroxide octahydrate (97% active) are suspended in one liter of water at 50° C. temperature and stirred for 30 minutes at 50° C. followed by 60 minutes of agitation at 70° C. The hollow formed granulate is filtered and dried. The content of free fatty acid amounts to 1.7%.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04235794uspto-grants-1980_11