반응 #310937

ord-fab06d8802f34d2882e5fc578177755c

반응 조건

온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타to react them for 6 hours
  2. 2
    온도The reaction product was cooled to 80° C.

실험 절차

A mixture of 3.3 g of 2-mercaptobenzothiazole and 10.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C. and then 30 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzothiazolium p-toluenesulfonate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04356247uspto-grants-1982_10