반응 #310936

ord-6d3676ef55cf40839f114250a86a744b

반응 방정식

CCO
ethanol
CCO
ethanol
Sc1nc2ccccc2o1
2-mercaptobenzoxazole
CCOS(=O)(=O)c1ccc(C)cc1
ethyl p-toluenesulfonate
CCSc1oc2ccccc2[n+]1CC.Cc1ccc(S(=O)(=O)O)cc1
2-ethylmercapto-3-ethylbenzoxazolium p-toluenesulfonate

반응 조건

온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타to react them for 6 hours
  2. 2
    온도The reaction product was cooled to 80° C.

실험 절차

A mixture of 3.0 g of 2-mercaptobenzoxazole and 12.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C., and 25 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzoxazolium-p-toluenesulfonate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04356247uspto-grants-1982_10