반응 #310936
ord-6d3676ef55cf40839f114250a86a744b
반응 방정식
ethanol
ethanol
2-mercaptobenzoxazole
ethyl p-toluenesulfonate
→
2-ethylmercapto-3-ethylbenzoxazolium p-toluenesulfonate
반응 조건
온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타to react them for 6 hours
- 2온도The reaction product was cooled to 80° C.
실험 절차
A mixture of 3.0 g of 2-mercaptobenzoxazole and 12.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C., and 25 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzoxazolium-p-toluenesulfonate.