반응 #310736

반응 방정식

methyl dichlorosilane

1-decene

→

methyl decyl dichlorosilane

수율 94.0%

용매

2-propanol

반응 조건

후처리

1. 1
   workup.ADDITIONwere charged to a reaction vessel
2. 2
   온도heated to about 100°-120° C. for six hours
3. 3
   workup.DISTILLATIONdistilled at 110°-114° C. at 1-3 Torr

실험 절차

2.25 Parts of methyl dichlorosilane, 4.04 parts of 1-decene and a solution containing about 0.0005 part of chloroplatinic acid catalyst in 0.006 part of 2-propanol were charged to a reaction vessel and heated to about 100°-120° C. for six hours. The product was vacuum distilled at 110°-114° C. at 1-3 Torr. 4.7 Parts (94% yield) of methyl decyl dichlorosilane was obtained.

출처