반응 #310707

반응 방정식

acryloyl chloride

alanine ethyl ester hydrochloride

sodium carbonate

→

N-acryloylalanine ethyl ester

용매

benzene

반응 조건

후처리

1. 1
   온도The reaction mixture is then refluxed for 1 hour
2. 2
   여과filtered
3. 3
   농축the filtrate concentrated

실험 절차

To 0.5 moles of alanine ethyl ester hydrochloride in 500 ml. of benzene is added 0.5 moles of acryloyl chloride. To this stirred mixture is added portionwise 0.6 moles of anhydrous sodium carbonate. The reaction mixture is then refluxed for 1 hour, stirred an additional 2 hours, filtered, and the filtrate concentrated to give N-acryloylalanine ethyl ester.

출처