반응 #3072

ord-136efa4c469642d7aa6076afa6f445aa

반응 방정식

COC(=O)c1ccc(O)cc1
methyl 4-hydroxybenzoate
C=CCBr
allyl bromide
O=C([O-])[O-].[K+].[K+]
K2CO3
→
C=CCOc1ccc(C(=O)OC)cc1
methyl 4-allyloxybenzoate

반응물

COC(=O)c1ccc(O)cc1
methyl 4-hydroxybenzoate
C=CCBr
allyl bromide
O=C([O-])[O-].[K+].[K+]
K2CO3

시약

없음

용매

CC(C)=O
acetone

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    추출Extraction

실험 절차

A mixture of 1.0 mmol of methyl 4-hydroxybenzoate, 2.0 mmol of allyl bromide, 5.0 mmol of K2CO3 in 2 mL of acetone was stirred for 16 h. Extraction provided methyl 4-allyloxybenzoate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05731432uspto-grants-1998_03