반응 #3070

반응 방정식

aldehyde

3-iodo-4-methylbenzaldehyde

n-BuLi

→

3-iodo-4-methylstyrene

용매

THF

반응 조건

후처리

1. 1
   추출processed by extraction and chromatography

실험 절차

This aldehyde (1 mmol)was added to a premixed solution of 1.5 mmol of methyl triphenylphosphonium bromide and 1.2 mmol of n-BuLi in 5 mL of THF at 0° C. and this mixture was stirred for 3-6 h at rt and then processed by extraction and chromatography to give 3-iodo-4-methylstyrene.

출처