반응 #3064
ord-2f2ad81b1f6b433ea7c984999ad32978
반응 방정식
phenylalanine methyl ester hydrochloride
triethylamine
formic acid
acetic anhydride
→
N-formylphenylalanine methyl ester
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
To a mixture of 1 mmol of phenylalanine methyl ester hydrochloride and 2 mmol of triethylamine in 1 mL of DMF at 0 ° C. was added 2 mL of formic acid and 0.7 mL of acetic anhydride. After stirring for 16 h at rt, extractive isolation provided N-formylphenylalanine methyl ester.