반응 #3062
ord-53859d19f5084c73a9229630dac0c84d
반응 방정식
iminodiacetic acid dimethylester hydrochloride salt
N,N-diisopropyl-ethylamine
1,3-dibromopropane
→
title compound
Dimethyl N-(3-Bromopropyl)iminodiacetate
시약
없음
용매
반응 조건
온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타chromatographed
실험 절차
A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.